Variable Temperature Sample Environment Summary
Equipment | Sample type | Temperature range and operating units | Ramp rate limits and units | Setup time (hrs) (includes normal beamline setup) | Other info | Which column in a .parab file is the temperature? |
Serpentine hot air blower  | Broken quartz capillary | Room Temperature - 750°C | 50°/minute heating or cooling | 5 | Users should do their own calibration | SR10BM01HU02IOC01:ET:RBV_pvTemp 0 Eurotherm_Temperature_(C) |
|
|
|
|
|
|
|
Cyberstar hot air blower  | Broken quartz capillary | Room Temperature - 950°C | 6°/minute heating, 15°/minute cooling | 5 | Temperature calibration exists | SR10BM01HU02IOC01:ET:RBV_pvTemp 0 Eurotherm_Temperature_(C) |
|
|
|
|
|
|
|
Oxford Cryosystems Cryostream | Broken quartz capillary | 80 - 480 K | 360°/hour (6°/min) | 5 | Equipment is calibrated | SR10BM01HU02IOC01:CS700:GAS_TEMP 0 Cryo_Temperature_(K) |
|
|
|
|
|
|
|
Cryostat
| Capillary (Aluminium) | 10 - 300K |
| 10 | Aluminium capillaries required, equipment is calibrated | SR10BM01HU02IOC01:CRY:KELVINA_MONITOR 0 Cryostat_Temperature_(K) |
|
|
|
|
|
|
|
Stoe Capillary Furnace | Quartz/Sapphire Capillary (full length - with funnel) | Room Temperature - 1200°C | 50°/minute heating or cooling | 10 | Users should do their own calibration - Kapton windows add to low angle background | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |
|
|
|
|
|
|
|
Anton Paar DHS 1100
| Flat sample/powder | Room Temperature - 1100°C | 50°/minute heating or cooling | 7 | Users should do their own calibration. Corrections to data required due to geometry. Sample chamber can be flooded with inert gas. | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |
|
|
|
|
|
|
|
Anton Paar HTK2000 | Flat sample/powder | Room Temperature - 1870 K, using a Pt filament and 2000K with W filament | 50°/minute heating or cooling | 10 | Users should do their own calibration. Corrections to data required due to geometry. Sample chamber can be flooded with inert gas. | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |