Variable Temperature Sample Environments

Variable Temperature Sample Environments

Equipment

Sample Type

Temperature Range

Ramp Rate Limits

Setup Time (hrs)

Other Info

Atmosphere

Serpentine hot air blower

Capillary

RT-700°C

Special glass and borosilicate (max 550°C), quartz capillary (max 1100°C)

50°min heating or cooling

5

Users should do their own calibration.

Vacuum (10-4mbar), N2, Ar, CO2, He and flammable gases such as H2 and CH4

Cyberstar hot air blower

Capillary

RT-950°C

Special glass and borosilicate (max 550°C), quartz capillary (max 1100°C)

6°min heating, 15°min cooling

5

Users should do their own calibration.

Vacuum (10-4mbar), N2, Ar, CO2, He and flammable gases such as H2 and CH4

Oxford Cryosystems Cryostream

Capillary

80-480K

360°h/6°min

 

5

Users should do their own calibration.

Vacuum, N2, Ar, CO2, He and flammable gases such as H2 and CH4

Cryostat

Aluminium capillary

10-300 K

4°min heating, 2.5°min cooling

8

Users need to purchase aluminium capillaries.

Users should do their own calibration.

No

Stoe Capillary Furnace

Capillary

RT-1200 °C

Special glass and borosilicate (max 550°C), quartz capillary (max 1100°C), sapphire capillary (>1100°C).

50°min heating or cooling

8

Users should do their own calibration.

No

Anton Paar DHS 1100

 

Flat sample/powder

RT-1100 °C

50°min heating or cooling

7

Users should do their own calibration.

Corrections to data required due to geometry.

Vacuum (10 -1 mbar), air,
He, Ar, N2

Anton Paar HTK2000

Flat sample/powder

RT-1870 K, using a Pt filament and 2000K with W filament

50°min heating or cooling

8

Users need to supply their own Pt strips.

Users should do their own calibration.

Corrections to data required due to geometry.

Vacuum (10-4mbar), air, He, Ar