Variable Temperature Sample Environment Summary
- Diffraction Cluster (Unlicensed)
- AS Diffraction Wiki
Equipment | Sample type | Temperature range and operating units | Ramp rate limits and units | Setup time (hrs) (includes normal beamline setup) | Other info | Which column in a .asc file is the temperature? |
Serpentine hot air blower  | Broken quartz capillary | Room Temperature - 750°C | 50°/minute heating or cooling | 5 | Users should do their own calibration | SR10BM01HU02IOC01:ET:RBV_pvTemp 0 Eurotherm_Temperature_(C) |
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Cyberstar hot air blower  | Broken quartz capillary | Room Temperature - 950°C | 6°/minute heating, 15°/minute cooling | 5 | Temperature calibration exists | SR10BM01HU02IOC01:ET:RBV_pvTemp 0 Eurotherm_Temperature_(C) |
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Oxford Cryosystems Cryostream | Broken quartz capillary | 80 - 500 K | 360°/hour (6°/min) Time needed to cool from 300 K to 80 K: 1 h. | 5 | Equipment is calibrated | SR10BM01CS800:CURRENTTEMPERATURE |
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Cryostat
| Capillary (Aluminium) | 10 - 300K | 4°/minute heating, 2.5°/minute cooling Time needed to cool from 300 K to 10 K: 2 h 15 m. | 10 | Aluminium capillaries required, equipment is calibrated | SR10BM01HU02IOC01:CRY:KELVINA_MONITOR 0 Cryostat_Temperature_(K) |
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Stoe Capillary Furnace | Quartz/Sapphire Capillary (full length - with funnel) | Room Temperature - 1200°C | 50°/minute heating or cooling | 10 | Users should do their own calibration - Kapton windows add to low angle background | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |
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Anton Paar DHS 1100
| Flat sample/powder | Room Temperature - 1100°C | 50°/minute heating or cooling | 7 | Users should do their own calibration. Corrections to data required due to geometry. Sample chamber can be flooded with inert gas. | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |
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Anton Paar HTK2000 | Flat sample/powder | Room Temperature - 1870 K, using a Pt filament and 2000K with W filament | 50°/minute heating or cooling | 10 | Users should do their own calibration. Corrections to data required due to geometry. Sample chamber can be flooded with inert gas. | SR10BM01HU02IOC01:FRNC:RBV_pvTemp 0 Furnace_Temperature_(C) |