Main Experimental Hutch (Hutch B)
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A capillary set up and hot air blower from the Powder Diffraction Beamline is pictured below. Please note that because this resource is shared between beamlines, availability is not guaranteed. This is used for variable temperature experiments up to 700°C (this upper limit may be lower for certain flammable gases such as H2), and/or where samples are maintained under a specific gas atmosphere either as flow-through or under pressure up to a maximum of 20 bar. The beamline delivers gas through 6 mm nylon tubes. Please note that these are rated to 10 bar only. If working at pressures above 10 bringbar, bring your own steel lines.Please note that because this resource is shared between beamlines, availability is not guaranteed.
🧐Where can I purchase suitable capillaries?
Capillaries can be ordered from e.g. Hilgenberg or Charles Supper, and standard stock items will take at least two weeks to be delivered. For non-standard thicker-walled quartz capillaries, users will need to contact Hilgenberg directly for pricing and availability. Delivery time might be longer.
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max 3% H2 (in N2 balance) for temperature dependent measurements up o to max 400°C
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There is no dedicated gas extraction system in the hutches, consider bringing a gas collection bag that can be emptied in our fume hood post experiment. |
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