Page Comparison

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Capillary rack with 9 positions that will take standard 1.5 mm diameter capillaries (sample volume 80-200 µL) available from Hilgenberg/Charles Supper. Users are expected to supply their own capillaries for measurements using the capillary rack and the beamline team can supply the contact details of the relevant suppliers. Each capillary position is heated by a peltier element, providing temperature control within temperature ranges for standard measurements in aqueous solution (5-80 °C). Temperature-ramp schemes are programmable in sequence with data acquisition.

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Linkam Stage

A temperature-controlled stage with a single capillary position that takes standard 1.5 mm diameter capillaries (sample volume 80-200 µL) available from Hilgenberg/Charles Supper. Users are expected to supply their own capillaries. The Linkam Stage provides a wider temperature range, of up to 350 °C, for the measurements of fluid samples. Temperature-ramp schemes are programmable in sequence with data acquisition. The position of the capillary can be moved vertically to the beam during an acquisition sequence, enabling data collection at multiple positions along the sample.

Flowthrough Capillary

For dynamic measurements on evolving systems circulated through a capillary using a peristaltic pump. Sample volumes will need to be on the order of 15-20 mL to ensure sufficient volume for circulation though the capillary. Multiple modes of operation are possible with this sample environment including:

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